•  
  •  
 

Journal of Food Science and Biotechnology

Corresponding Author(s)

宋春芳(1974—),女,博士,教授,博士研究生导师,主要从事农产品无损检测与控制研究。E-mail:songcf@jiangnan.edu.cn

Abstract

[Objective ] This study aims to assess the quality of Tieguanyin oolong tea during the baking process.[Method ] Near-infrared spectroscopy was used for non-destructive detection of Tieguanyin oolong tea during the baking process and chemometrics was employed to analyze the changes in the intrinsic quality of the Tieguanyin oolong tea.Spectral preprocessing and dimensionality reduction were conducted for the near-infrared spectral data.Support vector machine (SVM ) and back propagation neural network (BPNN ) were adopted to construct discrimination models for the baking degree of Tieguanyin oolong tea.Combining the near-infrared spectral data with intrinsic quality data,partial least squares regression (PLSR ) was employed to build quality prediction models.[Result ] According to the changes in intrinsic quality and sensory evaluation results,the baking degree of Tieguanyin oolong tea can be graded into under baking,moderate baking,and over baking.Under the full-spectrum spectral data model,with preprocessing as multiple scatter correction (MSC ) and the discriminant model as BPNN,the discriminant effect was the best,and the accuracy rate of the test set was 100.00%.When predicting the four intrinsic quality properties,the prediction model combining the successive projections algorithm (SPA ) with PLSR had the best accuracy.The determination coefficients of prediction (R2P) of the best prediction model for free amino acids,tea polyphenols,catechins,and caffeine were 0.949 6,0.944 3,0.950 8,and 0.740 0,respectively.[Conclusion ] This study realized the accurate discrimination of the baking degree and the rapid prediction of quality of Tieguanyin oolong tea,providing a theoretical foundation for the accurate discrimination and control of oolong tea baking.

Publication Date

9-15-2025

First Page

153

Last Page

162

DOI

10.12441/spyswjs.20240919002

References

[1] BAG S,MONDAL A,MAJUMDER A,et al.Tea and its phytochemicals:hidden health benefits & modulation of signaling cascade by phytochemicals [J].Food Chemistry,2022,371:131098.
[2] 黄福平,叶乃兴.乌龙茶市场的现状与前景 [J].茶叶科学简报,1993,34(4):24-28.HUANG F P,YE N X.Status and prospects of oolong tea market [J].Acta Tea Sinica,1993,34(4):24-28.(in Chinese)
[3] 柳镇章.安溪铁观音产品品质及拼配、烘焙和贮存关键技术的研究 [D].福州:福建农林大学,2022.
[4] CAO Q Q,FU Y Q,WANG J Q,et al.Sensory and chemical characteristics of Tieguanyin oolong tea after roasting[J].Food Chemistry:X,2021,12:100178.
[5] 王飞,孙云,周子维,等.不同焙火程度对闽北乌龙茶化学品质的影响 [J].宁德师范学院学报 (自然科学版 ),2023,35(4):407-413.WANG F,SUN Y,ZHOU Z W,et al.Effects of different roasting degrees on the chemical quality of Minbei oolong tea[J].Journal of Ningde Normal University (Natural Science),2023,35(4):407-413.(in Chinese )
[6] 谢善锦.乌龙茶烘焙工艺现状及发展分析 [J].福建茶叶,2022,44(5):18-20.XIE S J.Analysis on present situation and development of oolong tea baking technology [J].Tea in Fujian,2022,44(5):18-20.(in Chinese )
[7] DIAZ-OLIVARES J A,VAN NUENEN A,GOTE M J,et al.Near-infrared spectra dataset of milk composition in transmittance mode [J].Data in Brief,2023,51:109767.
[8] WU X H,FANG Y H,WU B,et al.Application of near-infrared spectroscopy and fuzzy improved null linear discriminant analysis for rapid discrimination of milk brands[J].Foods,2023,12(21):3929.
[9] XIA H L,CHEN W,HU D,et al.Rapid discrimination of quality grade of black tea based on near-infrared spectroscopy (NIRS),electronic nose (E-nose) and data fusion[J].Food Chemistry,2024,440:138242.
[10] ZHANG Z Q,ZANG M W,ZHANG K H,et al.Effect of two types of thermal processing methods on the aroma and taste profiles of three commercial plant-based beef analogues and beef by GC-MS,E-nose,E-tongue,and sensory evaluation [J].Food Control,2023,146:109551.
[11] LI H H,SUN X,PAN W X,et al.Feasibility study on nondestructively sensing meat ’s freshness using light scattering imaging technique [J].Meat Science,2016,119:102-109.
[12] ZHANG Y,LI Z,WANG Q Y,et al.Rapid and visual evaluation the internal corruption of meat tissue by a designed near-infrared fluorescence probe with a broad pH response range [J].Spectrochimica Acta Part A:Molecular and Biomolecular Spectroscopy,2023,302:123035.
[13] OUACHA E H,LEGHRIB R,KHATIB N,et al.Ultrasound monitoring of water content in ultra high temperature milk [J].Instrumentation Mesure Métrologie,2023,22(4):177-183.
[14] YAN S H.Evaluation of the composition and sensory properties of tea using near infrared spectroscopy and principal component analysis [J].Journal of Near Infrared Spectroscopy,2005,13(6):313-325.
[15] TIAN Z X,TAN Z F,LI Y J,et al.Rapid monitoring of flavonoid content in sweet tea (Lithocarpus litseifolius (Hance) Chun) leaves using NIR spectroscopy [J].Plant Methods,2022,18(1):44.
[16] WANG S S,WU Z M,CAO C M,et al.Design and experiment of online detection system for water content of fresh tea leaves after harvesting based on near infra-red spectroscopy [J].Sensors,2023,23(2):666.
[17] REN G X,YIN L L,WU R,et al.Rapid detection of ash content in black tea using a homemade miniature near-infrared spectroscopy [J].Spectrochimica Acta Part A:Molecular and Biomolecular Spectroscopy,2024,308:123740.
[18] REN G X,ZHANG X S,WU R,et al.Digital depiction of the quality of Dianhong black tea based on pocket-sized near infrared spectroscopy [J].Infrared Physics & Technology,2022,127:104418.
[19] JIA J M,ZHOU X F,LI Y,et al.Establishment of a rapid detection model for the sensory quality and components of Yuezhou Longjing tea using near-infrared spectroscopy [J].LWT-Food Science and Technology,2022,164:113625.
[20] WU J Z,ZAREEF M,CHEN Q S,et al.Application of visible-near infrared spectroscopy in tandem with multivariate analysis for the rapid evaluation of matcha physicochemical indicators [J].Food Chemistry,2023,421:136185.
[21] DING Y H,YAN Y L,LI J,et al.Classification of tea quality levels using near-infrared spectroscopy based on CLPSO-SVM [J].Foods,2022,11(11):1658.
[22] SONG F H,HAO X,LI Z F,et al.Monitoring the baking quality of Tieguanyin via electronic nose combined with GC-MS[J].Food Research International,2023,165:112513.
[23] 葛诗蓓,金迪迪,杨明来,等.不同比例红蓝光对茶叶品质成分的影响与相关调控机理研究 [J].浙江农业学报,2022,34(10):2105 -2111.GE S B,JIN D D,YANG M L,et al.Effects and regulation mechanism of different proportions of red and blue light on quality components in tea (Camellia sinensis L.) plant[J].Acta Agriculturae Zhejiangensis,2022,34(10):2105 -2111.(in Chinese )
[24] 王秀英.福建乌龙茶咖啡碱含量分析及烘焙工艺研究[D].福州:福建农林大学,2009.
[25] 陈加友,高飞,冉琴,等.三段式烘焙工艺对安溪铁观音成茶品质的影响 [J].宁德师范学院学报 (自然科学版),2022,34(4):396-402.CHEN J Y,GAO F,RAN Q,et al.Effects of different three-stage baking processes on the quality of Anxi Tieguanyin tea [J].Journal of Ningde Teachers College (Natural Science ),2022,34(4):396-402.(in Chinese )
[26] LIU X B,LIU Y W,LI P,et al.Chemical characterization of Wuyi rock tea with different roasting degrees and their discrimination based on volatile profiles[J].RSC Advances,2021,11(20):12074 -12085.
[27] 唐雪平.基于化学分析与机器学习的铁观音茶叶品质评价体系 [D].泉州:华侨大学,2020.
[28] 付光明,高子婷,杨建新,等.基于近红外光谱的烤烟油分识别研究 [J].河南农业大学学报,2024,58(4):583-591.FU G M,GAO Z T,YANG J X,et al.Research on oil levels identification of flue-cured tobacco based on near infrared spectroscopy [J].Journal of Henan Agricultural University,2024,58(4):583-591.(in Chinese )
[29] ZHANG B,LI Z F,SONG F H,et al.Discrimination of black tea fermentation degree based on multi-data fusion of near-infrared spectroscopy and machine vision [J].Journal of Food Measurement and Characterization,2023,17(4):4149 -4160.
[30] WU T,ZHANG H M,XIAO Y X,et al.Quantification of multiple elements in Anji white tea using hyperspectral imaging combined with machine learning regression [J].Journal of Food Composition and Analysis,2025,142:107520.
[31] WANG Y J,JIN S S,LI M H,et al.Onsite nutritional diagnosis of tea plants using micro near-infrared spectrometer coupled with chemometrics [J].Computers and Electronics in Agriculture,2020,175:105538.
[32] GUO Z M,CHEN Q S,CHEN L P,et al.Optimization of informative spectral variables for the quantification of EGCG in green tea using Fourier transform near-infrared (FT-NIR) spectroscopy and multivariate calibration [J].Applied Spectroscopy,2011,65(9):1062 -1067.
[33] HUANG Y F,DONG W T,SANAEIFAR A,et al.Development of simple identification models for four main catechins and caffeine in fresh green tea leaf based on visible and near-infrared spectroscopy [J].Computers and Electronics in Agriculture,2020,173:105388.
[34] LUO W,TIAN P,FAN G Z,et al.Non-destructive determination of four tea polyphenols in fresh tea using visible and near-infrared spectroscopy [J].Infrared Physics & Technology,2022,123:104037.
[35] CHANDA S,HAZARIKA A K,CHOUDHURY N,et al.Support vector machine regression on selected wavelength regions for quantitative analysis of caffeine in tea leaves by near infrared spectroscopy [J].Journal of Chemometrics,2019,33(10):e3172.

Share

COinS
 
 

To view the content in your browser, please download Adobe Reader or, alternately,
you may Download the file to your hard drive.

NOTE: The latest versions of Adobe Reader do not support viewing PDF files within Firefox on Mac OS and if you are using a modern (Intel) Mac, there is no official plugin for viewing PDF files within the browser window.